Título:	Self-supported nickel nanoparticles on germanophosphate glasses : synthesis and applications in catalysis
Autor(es):	Lenz, Guilherme Felipe Schneider, Rodrigo Aguiar, Kelen M. F. Rossi de Bini, Rafael A. Chaker, Juliano Alexandre Hammer, Peter Botteselle, Giancarlo V. Felix, Jorlandio Francisco Schneider, Ricardo
Assunto:	Nanopartículas Níquel Catalisadores
Data de publicação:	31-Mai-2019
Editora:	Royal Society of Chemistry
Referência:	LENZ, Guilherme Felipe et al. Self-supported nickel nanoparticles on germanophosphate glasses: synthesis and applications in catalysis. RSC Advances, v. 9, n. 30, p. 17157–17164, 31 maio 2019. DOI: 10.1039/c9ra02927c. Disponível em: https://pubs.rsc.org/en/content/articlelanding/2019/ra/c9ra02927c#!divAbstract. Acesso em: 04 mar. 2020.
Abstract:	The development of supported catalysts based on simple procedures without waste products and timeconsuming steps is highly desirable. In this paper, self-supported nickel-based nanoparticles were obtained at the surface of the germanophosphate glasses by bottom-up process and evaluated as potential catalysts for the benzyl alcohol oxidation and bis(indolyl)methanes synthesis. A classical meltquenching technique was used for preparing the nickel-doped germanophosphate glasses, followed by annealing under a hydrogen atmosphere at 400 C for two different times. The approach enabled the synthesis of self-supported nanoparticles as a homogeneous film, covering the glass surface. The physical and chemical properties of synthesized glasses were characterized by UV-vis and Raman spectroscopies and thermal analysis. Scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS) were performed to monitor the growth process, morphology and chemical bonding structure of the nanoparticles surface.
Unidade Acadêmica:	Instituto de Química (IQ)
Licença:	(CC BY) - Open Access Article. Published on 31 May 2019. Downloaded on 2/28/2020 2:08:34 PM. This article is licensed under a Creative Commons Attribution 3.0 Unported Licence.
DOI:	10.1039/c9ra02927c
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